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Aging properties and aging mechanism of activated waste rubber powder modified asphalt binder based on

《结构与土木工程前沿（英文）》 2023年 第17卷 第4期   页码 625-636 doi: 10.1007/s11709-023-0938-1

摘要： The research and development of high-performance pavement materials has been intensified owing to the demand for long-life pavements. This study is performed to develop a novel pavement material using waste rubber powder, waste lubricating by-product (LBP), and asphalt. Subsequently, the aging properties and aging mechanism of activated waste rubber powder modified asphalt (ARMA) are investigated based on its rheological properties and micro-characterization. The rheological results show that, compared with waste rubber powder modified asphalt (RMA), ARMA offers a higher aging resistance and a longer fatigue life. A comparison and analysis of the rheological aging parameters of ARMA and RMA show that LBP activation diminishes the aging sensitivity of ARMA. The micro-characterization result shows that the aging of ARMA may be caused by the fact that LBP-activated waste rubber powder is more reactive and can form a dense colloidal structure with asphalt. Therefore, the evaporation loss of asphalt light components by heat and the damage to the colloidal structure by oxygen during the aging process are impeded, and the thermal-oxidative aging resistance of ARMA is improved.

关键词： rubber powder modified asphalt     aging     mechanism     rheological     characterization    

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Using thermodynamic parameters to study self-healing and interface properties of crumb rubber modifiedasphalt based on molecular dynamics simulation

Dongliang HU, Jianzhong PEI, Rui LI, Jiupeng ZHANG, Yanshun JIA, Zepeng FAN

《结构与土木工程前沿（英文）》 2020年 第14卷 第1期   页码 109-122 doi: 10.1007/s11709-019-0579-6

摘要： The thermodynamic property of asphalt binder is changed by the addition of crumb rubber, which in turn influences the self-healing property as well as the cohesion and adhesion within the asphalt-aggregate system. This study investigated the self-healing and interface properties of crumb rubber modified asphalt (CRMA) using thermodynamic parameters based on the molecular simulation approach. The molecular models of CRMA were built with representative structures of the virgin asphalt and the crumb rubber. The aggregate was represented by SiO and Al O crystals. The self-healing capability was evaluated with the thermodynamic parameter wetting time, work of cohesion and diffusivity. The interface properties were evaluated by characterizing the adhesion capability, the debonding potential and the moisture susceptibility of the asphalt-aggregate interface. The self-healing capability of CRMA is found to decrease as the rubber content increases. The asphalt-Al O interface with higher rubber content has stronger adhesion and moisture stability. But the influence of crumb rubber on the interfacial properties of asphalt-SiO interface has no statistical significance. Comparing with the interfacial properties of the asphalt-SiO interface, the asphalt-Al O interface is found to have a stronger adhesion but a worse moisture susceptibility for its enormous thermodynamic potential for water to displace the asphalt binder.

关键词： crumb rubber modified asphalt     surface free energy     self-healing     interface properties     molecular dynamics simulation    

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Evaluation of the compatibility between rubber and asphalt based on molecular dynamics simulation

Fucheng GUO, Jiupeng ZHANG, Jianzhong PEI, Weisi MA, Zhuang HU, Yongsheng GUAN

《结构与土木工程前沿（英文）》 2020年 第14卷 第2期   页码 435-445 doi: 10.1007/s11709-019-0603-x

摘要： Using of rubber asphalt can both promote the recycling of waste tires and improve the performance of asphalt pavement. However, the segregation of rubber asphalt caused by the poor storage stability always appears during its application. Storage stability of asphalt and rubber is related to the compatibility and also influenced by rubber content. In this study, molecular models of different rubbers and chemical fractions of asphalt were built to perform the molecular dynamics simulation. The solubility parameter and binding energy between rubber and asphalt were obtained to evaluate the compatibility between rubber and asphalt as well as the influence of rubber content on compatibility. Results show that all three kinds of rubber are commendably compatible with asphalt, where the compatibility between asphalt and cis-polybutadiene rubber (BR) is the best, followed by styrene-butadiene rubber (SBR), and natural rubber (NR) is the worst. The optimum rubber contents for BR asphalt, SBR asphalt, and NR asphalt were determined as 15%, 15%, and 20%, respectively. In addition, the upper limits of rubber contents were found as between 25% and 30%, between 20% and 25%, and between 25% and 30%, respectively.

关键词： rubber asphalt     compatibility     rubber content     molecular dynamics simulation    

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Outdoor aging of road asphalt and SBS modified asphalt

Li XIANG, Juan TU, Jian CHENG, Guohe QUE

《化学科学与工程前沿（英文）》 2011年 第5卷 第1期   页码 35-42 doi: 10.1007/s11705-010-0551-4

摘要： The process of performance degradation of road asphalt (RA) is regarded as aging. At present, better understanding of the thermal-oxidative aging of asphalt is achieved and the corresponding method to evaluate this process is developed; meanwhile, photo-oxidative aging (aging in an atmospheric environment, which is referred to as “outdoor aging” in this paper) of asphalt remains at the initial stages of scientific exploration. The outdoor natural ultraviolet (UV) aging of RA and SBS modified asphalt (SBSMA) are investigated in this study. The experimental results show that the basic performances of RA and SBSMA present similar change tendencies. The softening point increased, while the penetration and ductility decreased as the outdoor aging time passed by, and the 5°C ductility (ductility measured at 5°C) of SBSMA decreased very quickly. The group components of RA and SBSMA also change during UV aging. The content of asphaltene rose and that of aromatics and saturates decreased, while the content of resins changed insignificantly. Moreover, the Fourier transform infrared (FTIR) graphs show that the content of sulfoxide and carbonyl groups in RA and SBSMA increased significantly during the outdoor aging process.

关键词： asphalt     SBS     modified road asphalt     outdoor aging     ultraviolet    

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Effect of different high viscosity modifiers on rheological properties of high viscosity asphalt

《结构与土木工程前沿（英文）》 2021年 第15卷 第6期   页码 1390-1399 doi: 10.1007/s11709-021-0775-z

摘要： High viscosity asphalt (HVA) has been a great success as a drainage pavement material. However, the larger porosity of drainage asphalt mixtures weakens the cohesion and adhesion and leads to premature rutting, water damage, spalling and cracking. The purpose of this study was to investigate the rheological properties of HVA prepared using different high viscosity modifiers through conventional tests, Brookfield viscosity tests, dynamic shear rheometer tests and bending beam rheometer tests. The conventional performance results demonstrated SBS + rubber asphalt (SRA-1/2) exhibited excellent elastic recovery and low-temperature flexibility. The 60°C dynamic viscosity results indicated TPS + rubber asphalt (TRA) had the excellent adhesion. The rotational viscosity results and rheological results indicated that SRA-2 not only exhibited excellent temperature stability and workability, as well as excellent resistance to deformation and rutting resistance, but also exhibited excellent low-temperature cracking resistance and relaxation performance. Based on rheological results, the PG classification of HVA was 16% rubber + asphalt for PG76-22, 20% rubber + asphalt for PG88-22, TRA and SRA-1/2 for PG88-28. From comprehensive evaluation of the viscosity, temperature stability and sensitivity, as well as high/low temperature performance of HVA, SRA-2 was found to be more suited to the requirements of drainage asphalt pavement materials.

关键词： high viscosity asphalt     rheological properties     rubber     modifier     viscosity    

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Effect of carbon black on the dynamic moduli of asphalt mixtures and its master curves

Chuangmin LI, Fanbo NING, Yuanyuan LI

《结构与土木工程前沿（英文）》 2019年 第13卷 第4期   页码 918-925 doi: 10.1007/s11709-019-0526-6

摘要： Modulus is one of the main parameters during the design of asphalt pavement structure, the newest specifications of China gives the dynamic moduli ranges of commonly used asphalt mixtures with base asphalt (BA) or styrene-butadiene-styrene modified asphalt (SBS MA), while the moduli ranges of mixtures with carbon black modified asphalt (CB MA) are not recommended. To investigate the CB effect on the dynamic moduli of CB MA mixtures, one commonly used asphalt mixture (AC-20) was designed with BA, SBS MA, and CB MA, respectively. Then, the uniaxial compression dynamic modulus tests were conducted at different temperatures and loading frequencies, the master curves of asphalt mixtures were analyzed based on the time-temperature equivalence principle. The results show that ith increasing loading frequency, the temperature dependence of dynamic moduli of all asphalt mixtures tend to be less obvious. Both SBS and CB can decrease the temperature sensitivity of asphalt mixture, the SBS MA mixture has the lowest temperature sensitivity, followed by CB MA and BA mixture. In addition, CB and SBS can obviously improve the dynamic modulus of the BA mixture, enhance the anti-deformation performance of pavement structure, and the improvement effect of CB is almost the same with SBS.

关键词： dynamic modulus     carbon black     master curve     modified asphalt     asphalt mixture    

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Green Road Construction Technologies in Guangzhou

Guan-feng An,Wen-yuan Huang,Jing-feng Zhang

《工程管理前沿（英文）》 2016年 第3卷 第1期   页码 80-86 doi: 10.15302/J-FEM-2016002

摘要： Total road pavement in Guangzhou reaches 77 ×10 m . Its huge maintenance and potential rehabilitation calls for a green road system. This paper presents a discussion, first about green road construction technologies together with their applications and development like reclaimed asphalt pavement, rubberized asphalt pavement, and warm mix asphalt; and then, about the key obstacles for promotion and activities, primarily for green road promotion, in the perspectives of the current technical and application situations in China and separately in Guangzhou. Based on environmental and conditional analysis, as well as a development expectation from an industrial viewpoint, this paper creates a development trend of green road technologies.

关键词： road     green construction     recycling of waste asphalt     rubber asphalt    

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Laboratory investigation of emulsified asphalt binder modified with wood-derived nano-cellulose and nano

Yunge WEI; Jiayu WANG; Ruoyu LI; Ling XU; Feipeng XIAO

《结构与土木工程前沿（英文）》 2022年 第16卷 第11期   页码 1474-1485 doi: 10.1007/s11709-022-0869-2

摘要： Emulsified asphalt is the primary material for preventive maintenance and cold-mix paving, but its low cohesive strength and poor mechanical properties limit its wide application, even with polymer modification. In this study, Styrene-Butadiene Rubber (SBR) emulsified asphalt was modified with nano-cellulose materials, namely nano paper-cellulose (NPC) and wood-derived nano-cellulose (WDC), to improve its properties. A novel preparation method of nano-cellulose solution was developed, including blending, ultrasonic stirring, and centrifugal treatment. Four types of nano-cellulose solution (0.5% NPC, 0.5%, 1.0%, and 1.5% WDC by weight of water) were selected. The microscopy analysis indicated that 0.5% WDC emulsion had a smaller particle size than 1.5% WDC emulsion. The rheology test indicated that WDC modified residue improved rutting resistance with the increased solution dosage due to the cross-linking effect, but its creep-and-recovery performance was worse than that of SBR emulsion residue. The NPC modified binder had a higher rutting factor than WDC modified binder at the same dosage after short-term aging. In addition, 1.0% WDC could be regarded as the optimal dosage in terms of fatigue and low-temperature performance. Furthermore, Fourier Transform Infrared Spectroscopy (FTIR) results showed that 0.5% NPC modified residue performed better in long-term aging resistance compared with 0.5%WDC modified asphalt.

关键词： nano-cellulose     emulsified asphalt binder     dispersion     rheological properties     Fourier transform infrared spectroscopy    

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新型高黏度改性沥青的研发和应用

杨林江

《中国工程科学》 2008年 第10卷 第12期   页码 92-96

摘要：

针对杭州湾大桥桥面铺装对高黏度改性沥青的技术要求，研发了一种新型高黏度改性沥青［1］。通过分析基质沥青、SBS、化学助剂的红外光谱，在研究沥青改性过程中微观结构变化规律的基础上，提出了采用SBS加化学接枝反应剂（增黏剂）TW-1和增容剂TW-2的沥青改性配伍设计，使改性沥青在提高低温延度、弹性恢复能力的同时，大幅度提升了60 ℃动力黏度，而施工和易性不受影响，产品在杭州湾大桥工程中得到了成功的应用。

关键词： 杭州湾大桥     高黏度改性沥青     配伍机理     红外光谱分析     路用性能     施工性能    

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Linear viscoelastic behavior of asphalt binders and mixtures containing very high percentages of reclaimedasphalt pavement

《结构与土木工程前沿（英文）》   页码 1211-1227 doi: 10.1007/s11709-023-0983-9

摘要： The primary aim of this study is to correlate the impact of aggregates, if any, on the viscoelastic behavior of rejuvenated asphalt mixtures containing very high amounts of reclaimed asphalt pavement (RAP) (> 50%). First, gradation of 100% RAP was rectified, using a modified Bailey method by adding virgin aggregates to achieve two coarse dense-graded and one fine dense-graded blends. Complex modulus test was then performed from −35 to +35 °C and 0.01–10 Hz. In addition to performance grade (PG) testing, extracted and recovered binders from different asphalt mixtures underwent shear complex modulus test within −8 °C to high temperature PG and frequencies from 0.001 to 30 Hz. Cole−Cole, Black space, complex modulus and phase angle master curves were constructed and Shift-Homothety-Shift in time-Shift (SHStS) transformation was used to compare the linear viscoelastic behavior of asphalt binders and mixtures. The influence of aggregates on the viscoelastic behavior of asphalt mixtures depends on temperature and/or frequency. The role of asphalt binders in the behavior of asphalt mixtures is more pronounced at high temperatures and the effect of the aggregate structure increases as the temperature falls. The maximum difference (60% to 70%) in the viscoelastic behavior of the binder and mixture based on SHStS transformed Cole−Cole curves is within the phase angle of 15°–20°.

关键词： RAP     complex modulus     SHStS transformation     rejuvenation     behavior of asphalt binder and mixture    

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Parametric study on seismic performance of self-centering reinforced concrete column with bottom-placed rubber

《结构与土木工程前沿（英文）》   页码 1145-1162 doi: 10.1007/s11709-023-0945-2

摘要： To realize seismic-resilient reinforced concrete (RC) moment-resisting frame structures, a novel self-centering RC column with a rubber layer placed at the bottom (SRRC column) is proposed herein. For the column, the longitudinal reinforcement dissipates seismic energy, the rubber layer allows the rocking of the column, and the unbonded prestressed tendon enables self-centering capacity. A refined finite element model of the SRRC column is developed, the effectiveness of which is validated based on experimental results. Results show that the SRRC column exhibits stable energy dissipation capacity and no strength degradation; additionally, it can significantly reduce permanent residual deformation and mitigate damage to concrete. Extensive parametric studies pertaining to SRRC columns have been conducted to investigate the critical factors affecting their seismic performance.

关键词： seismic resilience     self-centering     rubber layer     flag-shaped hysteresis loop     parametric study    

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Development and road performance of clear asphalt with high transparency and adhesion

《结构与土木工程前沿（英文）》 2023年 第17卷 第2期   页码 238-255 doi: 10.1007/s11709-022-0898-x

摘要： Clear asphalt (CA) currently used in light-colored asphalt mixtures (LCAM) exhibits poor transparency and adhesion. Therefore, a highly transparent CA (HCA) modified using a silane coupling agent (KH550) was prepared. Furthermore, LCAM was prepared by mixing CA and limestone aggregates. The properties of the HCA and ordinary CA (OCA) were characterized using conventional asphalt tests, optical tests, pull-off tests, ultraviolet aging tests, dynamic shear rheometry, Fourier-transform infrared spectroscopy, differential scanning calorimetry, and scanning electron microscopy. Whereas Marshall, moisture resistance, wheel tracking, trabecular bending, and British pendulum tests were employed for the LCAM. The transmittance and spectral reflectance of the HCA were 123.30 and 3.74 times greater than those of the OCA, respectively. The complex modulus and viscosity-aging index of the HCA were 48% and 53% less than those of the OCA, respectively. After modification with KH550, the Marshall stability ratio, tensile strength ratio, and flexural strain of the HCA-prepared LCAM increased by 12.92%, 25.06%, and 23.90%, respectively. However, the rutting resistance of the HCA-prepared LCAM was 14.3% less than that of the OCA-prepared LCAM. The comprehensive performances of the HCA and HCA-prepared LCAM were 49.2% and 10.3% greater than those of the OCA and OCA-prepared LCAM, respectively, indicating a high application value in the future.

关键词： light-colored asphalt pavement     orthogonal test     road performance     spectral reflectance     silane-coupling agent    

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Fatigue of asphalt binder, mastic and mixture at low temperature

Dong WANG, Linbing WANG, Guoqing ZHOU

《结构与土木工程前沿（英文）》 2012年 第6卷 第2期   页码 166-175 doi: 10.1007/s11709-012-0157-7

摘要： The fatigue damage is one of the most common distresses observed on the asphalt concrete pavement. To thoroughly understand the fatigue of asphalt concrete, the behaviors of the major components of asphalt concrete under cyclic loading are investigated respectively in this study. A new experiment method is developed to evaluate the performances of asphalt binder, mastic and fine aggregates mixture under cyclic tensile loading. The fatigue test results of asphalt binder show that the fatigue performance of asphalt binder is closely related with loading magnitude, temperature and loading rate. Mastic specimens with different filler content are tested and the results indicate that mastic specimens with 30% filler content show better fatigue resistance and higher permanent strain. The micro-structure analysis of mastic and mixture indicates that the fatigue resistance is closely related with the air void content of specimen. 3D digital specimens are developed to model the fatigue of the asphalt binder, mastic and mixture specimens based on the finite element method (FEM). Fatigue damage of asphalt concrete is simplified by a damage model. With proper selection of damage parameters, the simulation results agree well with laboratory test results and can be used as a basis for future fatigue research.

关键词： fatigue     asphalt mixture     asphalt binder     mastic     finite element method (FEM)     X-ray tomography    

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Effect of styrene-butadiene-styrene copolymer on the aging resistance of asphalt: An atomistic understanding

《结构与土木工程前沿（英文）》 2021年 第15卷 第5期   页码 1261-1276 doi: 10.1007/s11709-021-0761-5

摘要： To reveal the potential influence of styrene-butadiene-styrene (SBS) polymer modification on the anti-aging performance of asphalt, and its mechanism, we explored the aging characteristics of base asphalt and SBS-modified asphalt by reaction force field (ReaxFF) and classical molecular dynamics simulations. The results illustrate that the SBS asphalt is more susceptible to oxidative aging than the base asphalt under oxygen-deficient conditions due to the presence of unsaturated C=C bonds in the SBS polymer. In the case of sufficient oxygen, the SBS polymer inhibits the oxidation of asphalt by restraining the diffusion of asphalt molecules. Compared with the base asphalt, the SBS asphalt exhibits a higher degree of oxidation at the early stage of pavement service and a lower degree of oxidation in the long run. In addition, SBS polymer degrades into small blocks during aging, thus counteracting the hardening of aged asphalt and partially restoring its low-temperature cracking resistance.

关键词： SBS asphalt     oxidative aging     asphalt hardening     ReaxFF     molecular dynamics    

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Orientation effect of electropolishing characteristics of 316L stainless steel fabricated by laser powder

《机械工程前沿（英文）》 2021年 第16卷 第3期   页码 580-592 doi: 10.1007/s11465-021-0633-7

摘要： 3D metal printing process has attracted increasing attention in recent years due to advantages, such as flexibility and rapid prototyping. This study aims to investigate the orientation effect of electropolishing characteristics on different surfaces of 316L stainless steel fabricated by laser powder bed fusion (L-PBF), considering that the rough surface of 3D printed parts is a key factor limiting its applications in the industry. The electropolishing characteristics on the different surfaces corresponding to the building orientation in selective laser melting are studied. Experimental results show that electrolyte temperature has critical importance on the electropolishing, especially for the vertical direction to the layering plane. The finish of electropolished surfaces is affected by the defects generated during L-PBF process. Thus, the electropolished vertical surface has higher surface roughness Sa than the horizontal surface. The X-ray photoelectron spectroscopy spectra show that the electropolished horizontal surface has higher Cr/Fe element ratio than the vertical surface. The electropolished horizontal surface presents higher corrosion resistance than the vertical surface by measuring the anodic polarization curves and fitting the equivalent circuit of experimental electrochemical impedance spectroscopy.

关键词： electropolishing     laser powder bed fusion     316L stainless steel     corrosion resistance     microstructure    

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标题 作者 时间 类型 操作

Aging properties and aging mechanism of activated waste rubber powder modified asphalt binder based on

期刊论文

Using thermodynamic parameters to study self-healing and interface properties of crumb rubber modifiedasphalt based on molecular dynamics simulation

Dongliang HU, Jianzhong PEI, Rui LI, Jiupeng ZHANG, Yanshun JIA, Zepeng FAN

期刊论文

Evaluation of the compatibility between rubber and asphalt based on molecular dynamics simulation

Fucheng GUO, Jiupeng ZHANG, Jianzhong PEI, Weisi MA, Zhuang HU, Yongsheng GUAN

期刊论文

Outdoor aging of road asphalt and SBS modified asphalt

Li XIANG, Juan TU, Jian CHENG, Guohe QUE

期刊论文

Effect of different high viscosity modifiers on rheological properties of high viscosity asphalt

期刊论文

Effect of carbon black on the dynamic moduli of asphalt mixtures and its master curves

Chuangmin LI, Fanbo NING, Yuanyuan LI

期刊论文

Green Road Construction Technologies in Guangzhou

Guan-feng An,Wen-yuan Huang,Jing-feng Zhang

期刊论文

Laboratory investigation of emulsified asphalt binder modified with wood-derived nano-cellulose and nano

Yunge WEI; Jiayu WANG; Ruoyu LI; Ling XU; Feipeng XIAO

期刊论文

新型高黏度改性沥青的研发和应用

杨林江

期刊论文

Linear viscoelastic behavior of asphalt binders and mixtures containing very high percentages of reclaimedasphalt pavement

期刊论文

Parametric study on seismic performance of self-centering reinforced concrete column with bottom-placed rubber

期刊论文

Development and road performance of clear asphalt with high transparency and adhesion

期刊论文

Fatigue of asphalt binder, mastic and mixture at low temperature

Dong WANG, Linbing WANG, Guoqing ZHOU

期刊论文

Effect of styrene-butadiene-styrene copolymer on the aging resistance of asphalt: An atomistic understanding

期刊论文

Orientation effect of electropolishing characteristics of 316L stainless steel fabricated by laser powder

期刊论文